Friday, February 17, 2012

Projector HID arc light mounted into a desk lamp



I combined the High Intensity Discharge bulb and power supply from an old LCD with a desk lamp to create a 270W spotlight. I bypassed the power supply's interlocks and shorted an optocoupler to cause the power supply to always turn the lamp on when AC power is applied. I used an inline power switch to control the device. The desk lamp's existing wiring is able to withstand the high starting voltage of the HID lamp (probably a few KV). Once the arc strikes, the voltage is much lower and the current much higher.

Sunday, January 29, 2012

Freeze-drying Jello gelatin with an improved cold trap



I built an improved cold trap from an aluminum pan and a stainless steel bowl. It held more ice than my original copper pipe cold trap, but the 100ml of water from the gelatin still managed to almost plug up the trap.

Yeast cells under the microscope



These bakers' yeast cells might be reproducing in the video. It's hard to tell if its just movement from the water under the cover slip

Creating aerogel with supercritical methanol



In previous videos, I used supercritical CO2 to dry my homemade aerogels. This time, I soaked the aerogel in methanol, then raised the temperature and pressure of the methanol itself to make it supercritical. This allows the gels to be dried without an additional solvent exchange into CO2. The downside is that it requires a chamber full of methanol at 460*F and over 1200 psi, which is a much bigger hazard than using CO2.

The aerogels dried with methanol shrank less than the ones dried with CO2, but there was still a lot of cracking, and I have yet to create a high-quality monolith.

Thursday, January 12, 2012

Extracting caffeine with methylene chloride



In a previous video, I showed how to extract caffeinated water from green coffee beans with supercritical CO2. Here, I show how to extract dry caffeine crystals from the caffeinated water (ie coffee, in this case). I used a vacuum filtration setup to create very strong coffee, then mixed it with methylene chloride in a seperatory funnel. The methylene chloride sinks below the water, taking most of the caffeine with it. By opening the funnel carefully, only the methylene chloride and caffeine can be transferred to a flask where the methylene chloride is boiled away. I then mounted a test tube in a rubber stopped and filled the tube with ice. With the stopped in the flask, I evacuated the flask and applied heat. The caffeine will sublimate and collect on the cold test tube. I scraped off the caffeine and measured the mass.