Monday, May 7, 2012
Whipped chocolate made with high pressure nitrous oxide
I made some whipped chocolate by melting standard semi-sweet morsels, and applying nitrous oxide at 250 psi. I then dispensed the melted, gassified chocolate into a chilled vacuum chamber, then applied a vacuum to create large bubbles within the chocolate. I maintained the vacuum level while the chocolate solidified with the bubbles still intact. This process yields a dessert that is very low-density, and has a very pleasant airy texture.
Simple cloud chamber
A cloud chamber shows alpha particles being emitted from americium sources. The chamber works by creating a layer of supersaturated alcohol vapor which visualize the radation. The alpha particles trigger condensation in trails through the vapor cloud and show up as tiny droplet tracks. In this chamber, I have two alcohol-soaked pads above an aluminum plate that is cooled by dry ice. The pads emit alcohol vapor, which is cooled by the air above the aluminum plate to the point where it is colder than would normally by necessary to condense. The tiny radioactive particle pushes it over the edge to cause condensation, which is visible droplets.
Monday, April 30, 2012
Dissolving lithium in anhydrous ammonia
Here's an interesting reaction where lithium metal is dissolved in anhydrous ammonia. I placed a couple small pieces of lithium in a test tube, then connected the tube to a larger flask of ammonium hydroxide via silicone tubing. Upon heating the flask, gaseous ammonia will be produced which is condensed in the test tube by cooling it with a bath of alcohol and dry ice. The resulting solution is brilliant bronze in color, but at lower lithium concentrations, the solution is deep blue -- a very beautiful reaction.
Labels:
ammonia,
anhydrous ammonia,
dissolve,
dissolve lithium,
lithium
Monday, April 16, 2012
Lithium sheet metal and zirconium powder
I found some interesting materials at a local fleamarket (http://www.electronicsfleamarket.com/): a canister of lithium sheet metal, and a bottle of fine zirconium powder (325 mesh). The zirconium is stored under water since the dry power can self-ignite, or may be ignited by static electricity or shock. Confusingly, the MSDS sheets say that dry zirconium powder must not be allowed near water, but http://www.blogger.com/img/blank.gifif it is to be stored, it must be completely submerged in water. I carefully dried a very small amount, and sprinkled it over a flame.
If you know of something interesting to do with these chemicals, please let me know.
If you know of something interesting to do with these chemicals, please let me know.
Labels:
burn,
burning,
lithium,
zirconium,
zirconium powder
Tuesday, April 10, 2012
Making Pop Rocks candy at home
Here I show how I made gassified candy (eg Pop Rocks) in my home shop. The basic procedure is to heat sugar water up to 280*F, carbonate it with 600 psi CO2 and vigorous mixing, then cool the mixture while it is still under pressure. After the mixture has solidified, rapid depressurization causes the candy to burst apart into small fragments. Each fragment has lots of tiny CO2 bubbles embedded in it. When placed on the tongue, the bubbles burst open as the candy dissolves and a popping sensation is felt.
The main difficulty is building a high-pressure chamber that allows precise temperature control as well as thorough mixing of its contents while under pressure. I've built something that meets these requirements, and I've finally made a batch of candy that would pass as Pop Rocks, but they are pretty weak. I still need to adjust the temperature and mixing times to get a better product.
Link to recipe: http://www.exploratorium.edu/cooking/candy/recipe-lollipops.html
Labels:
candy,
DIY,
home shop,
make pop rocks,
making,
pop rocks,
poprocks,
sugar candy
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